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- W2079188875 abstract "The reactions of the pentamethylcyclopentadienyl-osmium compound Cp∗Os(NO)Br2 (1) with Na2S4 and (NEt4)2Se6 in dimethyl- formamide solution lead to mononuclear tetrachalcogenido complexes Cp∗ Os(NO) (E4) (E = S (2a), Se (2b)), whereas binuclear products Cp2∗Os2(NO)2(μ-E)2 (E = S (3a), Se (3b), Te (3c)) are obtained from the reactions of 1 with Li2E in tetrahydrofuran solution. Dechalcogenation of 2a,b using tri(n-butyl)phosphane gives 3a,b. The molecular geometry of Cp ∗ Os(NO)(Se4) (2b) has been determined by an X-ray crystal structure analysis which confirms the presence of a non-planar cyclotetraselenido chelate ligand." @default.
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- W2079188875 date "1996-07-01" @default.
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- W2079188875 title "The first Cp ∗ Os half-sandwich complexes containing chalcogenido ligands" @default.
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- W2079188875 doi "https://doi.org/10.1016/s0022-328x(96)06204-3" @default.
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