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- W2079208851 abstract "In this work attempt is made to study the crystallization, microstructure, and magnetic properties of a glass composition of 35% BaO, 35% Fe2O3, 20% B2O3, 10% SiO2 (mol%) without and with 1 mol% extra ZrO2 as nucleating agent, using various techniques. The formation of BaFe12O19 and BaB2O4 phases as the only crystalline phases formed in a glassy amorphous matrix were confirmed for all of the heat treated samples at their respective DTA exo-peak temperatures. Based on TEM, XRD and DTA results obtained, it was shown that the addition of ZrO2 promoted bulk crystallization in this system and also acted as a heterogeneous nucleation site for BaFe12O19 phase. Although, the magnitudes of the saturation magnetization (MS) of all of the heat treated samples were nearly in the same range (25-27 e.m.u./g), the values of the intrinsic coercive field (iHC) showed a mch wider range. The addition of ZrO2 to the glass system studied, have generally gave rise to the decrease of the iHC values. This is thought to be related to the substitution of non-magnetic Zr4+ions for Fe3+ in the barium hexaferrite lattice, weakening the superexhange interaction between Fe sites. The highest values of the iHC of the heat-treated base glass and ZrO2 added samples were 304 kA/m and 280kA/m, respectively. (© 2004 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
- W2079208851 created "2016-06-24" @default.
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- W2079208851 date "2004-12-01" @default.
- W2079208851 modified "2023-09-27" @default.
- W2079208851 title "Microstructural and magnetic properties of BaO-Fe2O3-B2O3-SiO2 glass ceramic with ZrO2 as nucleating agent" @default.
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- W2079208851 doi "https://doi.org/10.1002/pssc.200405422" @default.
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