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- W2079280990 abstract "Metal complexes ligated by 2-cyano- or 2-alkoxyimidate-1,10-phenanthrolines were synthesized. It was found that the alkoxyimidation of nitrile linked on ligand was speeded in metal complexes. In their ethylene oligomerization, manganese complexes were less active, cobalt complexes showed low to moderate activities, and nickel complexes gave moderate to good activities. The 2-alkoxyimidate-1,10-phenanthroline complexes of manganese, cobalt and nickel have been synthesized by the reaction of 2-cyano-1,10-phenanthroline with metal dichloride in the corresponding alcohol. The metal complexes bearing two 2-cyano-1,10-phenanthrolines were isolated in non-protonic solvent as the coordination around metal core with two ligands and two chlorides. The alkoxyimidation of nitrile linked on ligand was speeded in forming the 2-alkoxyimidate-1,10-phenanthrolinyl metal complexes. All the complexes have been characterized by FT-IR spectra and elemental analysis, and some of their structures have also been confirmed by single-crystal X-ray diffraction analysis. All the metal complexes were evaluated in the catalytic oligomerization of ethylene with some alkylaluminums as co-catalyst; in which manganese complexes were less active, cobalt complexes showed low to moderate activities, and nickel complexes gave moderate to good activities." @default.
- W2079280990 created "2016-06-24" @default.
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- W2079280990 date "2008-12-01" @default.
- W2079280990 modified "2023-10-14" @default.
- W2079280990 title "Transformation of 2-alkoxyimidate-1,10-phenanthroline metal (Mn2+, Co2+ and Ni2+) chlorides from bis(2-cyano-1,10-phenanthroline) metal chlorides: Syntheses, characterizations and their catalytic behavior toward ethylene oligomerization" @default.
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- W2079280990 doi "https://doi.org/10.1016/j.jorganchem.2008.09.052" @default.
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