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- W2079301577 abstract "A copper(II) complex with 6-hydroxypicolinic acid (6-OHpicH) and 3-picoline (3-pic), [Cu(6- OHpic)2(3-pic)2] (1), was prepared by recrystallization of [Cu(6-OHpic)2(H2O)2] from 3- picoline and characterized by IR spectroscopy and thermal methods (TGA/DTA and DSC). The molecular and crystal structure of 1 was determined by single-crystal X-ray structural analysis. The copper(II) ion in 1 has a tetragonally compressed octahedral coordination environment, achieved by two N, O-bidentate 6-hydroxypicolinate ligands and by two 3-picoline molecules in trans positions. The crystal structure of 1 exhibits one strong intermolecular O–H...O hydrogen bond, one weak intermolecular C–H...O hydrogen bond and one C– H...π interaction. Molecules of 1 are assembled into a 2D network in the (1 0 -1) plane, giving rise to C11(8) graph-set motif. These 2D networks are further assembled into 3D architecture only by weak Van der Waals interactions. A thermogravimetric study showed the initial loss of two coordinated 3-picoline molecules in 1, followed by a complete decomposition of the compound." @default.
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- W2079301577 date "2012-01-01" @default.
- W2079301577 modified "2023-10-03" @default.
- W2079301577 title "Synthesis and Characterization of a Copper(II) Complex with 6-Hydroxypicolinic Acid and 3-Picoline" @default.
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- W2079301577 doi "https://doi.org/10.5562/cca2119" @default.
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