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• W2079308020 startingPage "2397" @default.
• W2079308020 abstract "Four seven-co-ordinate manganese(II) complexes containing the ligand 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine (L1) have been synthesised by Schiff-base condensation of 2,6-diacetylpyridine and ethanolamine in the presence of Mn2+. A six-co-ordinate complex containing 2,6-bis[1-(3-hydroxypropylimino)ethyl]pyridine (L2) was obtained when the amine reagent was propanolamine. These complexes have been characterised by analytical, spectroscopic, magnetic, conductance, and single-crystal X-ray diffraction methods. Crystal data: [MnL1Cl2]·H2O (2), triclinic, a= 8.322(6), b= 8.465(5), c= 12.935(9)Å, α= 72.82(5), β= 72.20(6), γ= 81.38(5)°[{MnL2(NCS)2}x](5), monoclinic, a= 14.387(3), b= 10.045(2), c= 15.528(4)Å, and β= 115.10(2)°. The unusual seven-co-ordination observed is discussed in relation to the flexible non-cyclic ligands employed." @default.
• W2079308020 created "2016-06-24" @default.
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• W2079308020 date "1990-01-01" @default.
• W2079308020 modified "2023-10-10" @default.
• W2079308020 title "Six- and seven-co-ordinate manganese(<scp>II</scp>) complexes of Schiff-base ligands derived from the condensation of 2,6-diacetylpyridine with ethanolamine (L¹) or propanolamine (L²); X-ray crystal structures of [MnL¹Cl₂]·H₂O and [{MnL²(NCS)₂}_x]" @default.
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• W2079308020 doi "https://doi.org/10.1039/dt9900002397" @default.
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