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- W2079341496 abstract "Abstract Aluminophosphate molecular sieves (AlPO 4 's) were prepared by microwave heating without using organic template reagents. The microwave heating enhanced the crystallization of aluminophosphate gels, and AlPO 4 -H1, -H2(AHT), and -H3(APC) were successfully obtained as single phases in a relatively short reaction time. The reaction conditions used for the crystallization of the three kinds of AlPO 4 's were very similar to each other, but the use of different aluminum sources resulted in different structures; amorphous aluminum hydroxide, gibbsite, and boehmite were used for the preparation of AlPO 4 -H1, -H2, and -H3, respectively. The crystallization temperatures were 125, 118, and 90 °C, respectively. The addition of hydrochloric acid was needed for the crystallization of AlPO 4 -H1 and -H2. The addition of seed crystals and stirring the gels were found to be essential for the crystallization of AlPO 4 -H3. Nitrogen and water adsorption properties were also measured." @default.
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- W2079341496 date "2002-05-01" @default.
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- W2079341496 title "Template-free synthesis of AlPO4-H1, -H2, and -H3 by microwave heating" @default.
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- W2079341496 doi "https://doi.org/10.1016/s1387-1811(02)00314-1" @default.
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