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• W2079396352 abstract "An off-line 2-D-LC approach was developed for the separation and identification of components in extracts of Swertia franchetiana Smith, which is a traditional Chinese medicine. An octadecylsilica column was used for further separation of fractions from a cyano column with UV and MS detection. In this method, a longer column was used in the second dimension to improve the separation ability, and on-column focusing was adopted to reduce sample loss and pollution on concentrating the fractions from the first dimension. More than 118 and 575 components were detected in the chloroform and n-butanol extracts by this method, respectively. In contrast, only 20 and 95 peaks were detected by the one-dimensional method. Most of the additionally detected compounds were of low-abundance components. Many compounds can be preliminarily identified according to their UV and mass spectra in the two-dimensional method. The obtained results not only demonstrated the powerful resolution of 2-D-LC, but also led to in-depth comprehension of the UV and mass spectra of complex samples." @default.
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• W2079396352 date "2008-04-01" @default.
• W2079396352 modified "2023-10-14" @default.
• W2079396352 title "Two-dimensional LC-MS analysis of components inSwertia franchetianaSmith" @default.
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• W2079396352 doi "https://doi.org/10.1002/jssc.200700393" @default.
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