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• W2079403705 endingPage "1392" @default.
• W2079403705 startingPage "1385" @default.
• W2079403705 abstract "Hypercoordinated diorganotin(IV) dichloride, [2-(Et2NCH2)C6H4]2SnCl2 (1), was prepared by reacting [2-(Et2NCH2)C6H4]Li with SnCl4. Halide-exchange reactions between 1 and the appropriate potassium halides gave [2-(Et2NCH2)C6H4]2SnX2 [X = F (2), Br (3), I (4)]. Reaction of 1 with excess of Na2S gave the cyclo-[{2-(Et2NCH2)C6H4}2SnS]2 (5). The solution behavior of the title compounds in solution was investigated by multinuclear (1H, 13C, 19F and 119Sn) NMR spectroscopy, including variable temperature studies. Single-crystal X-ray diffraction analysis revealed for all compounds intramolecular N → Sn coordination thus resulting in distorted octahedral (C,N)2SnX2 configurations. Planar chirality is observed as result of the non-planarity of the SnC3N rings; all compounds, however, crystallizing as racemates. The isomers are linked by extensive hydrogen bonds to give different supramolecular architectures in the crystals of compounds 1, 3 and 4." @default.
• W2079403705 created "2016-06-24" @default.
• W2079403705 creator A5011775839 @default.
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• W2079403705 creator A5070555642 @default.
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• W2079403705 date "2009-04-01" @default.
• W2079403705 modified "2023-10-17" @default.
• W2079403705 title "Diorganotin(IV) compounds containing 2-(Et2NCH2)C6H4 moieties: Configurational stability in solution and solid state structures" @default.
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• W2079403705 doi "https://doi.org/10.1016/j.jorganchem.2008.12.023" @default.
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