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• W2079406037 abstract "A three phase junction: electrode|organic phase|aqueous phase is employed as microreactor for electrochemically assisted sol–gel silicate stripe deposition. A tin-doped indium oxide (ITO) electrode is immersed into the cell filled with two immiscible liquids. The aqueous phase on the top contains dissolved sodium sulphite salt whereas the organic phase on the bottom consists of sol–gel precursor solution–n-octyltriethoxysilane in a nitrobenzene. During electrochemical oxidation of the sulphite protons are generated in the aqueous phase. They act as catalyst for the sol–gel process of the precursor dissolved in the organic phase and a macroporous silicate stripe is formed at the electrode surface close to the three phase junction. Its size is controlled by the experimental conditions i.e. time of electrolysis. The smallest width of the obtained continuous structure is c.a. 10 μm." @default.
• W2079406037 created "2016-06-24" @default.
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• W2079406037 date "2008-10-01" @default.
• W2079406037 modified "2023-09-27" @default.
• W2079406037 title "Electrochemically assisted sol–gel process at a three phase junction" @default.
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• W2079406037 doi "https://doi.org/10.1016/j.elecom.2008.07.039" @default.
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