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- W2079425649 abstract "Abstract Thermal behavior of the Pb-substituted Bi-2223 phase was examined by characterizing samples annealed at 500°C to 850°C in air and also those subsequently reheated at 850°C in air by XRD, SEM and magnetic measurements. Very interesting reactions occurred, which were segregation of precipitates on annealing below 830°C and dissolution of the precipitates on subsequent reheating at 850°C into the 2223 phase. The precipitates were identified as Sr 2.5 Bi 0.5 Pb 3 Ca 2 CuO 2 . The precipitation and the dissolution were clearly confirmed by morphological observations of a fixed portion of a sample before and after heat treatments. These results strongly suggest that the 2223 phase changes its composition reversibly between the relatively Pb-rich composition stabilized above 850°C and relatively Pb-poor ones stabilized in essentially the same structure below 830°C. However, T c remained almost constant at 113 K." @default.
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- W2079425649 date "1994-01-01" @default.
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- W2079425649 title "Segregation and dissolution reactions of the 2223 phase in the Bi, Pb-Sr-Ca-Cu-O system on annealing in air" @default.
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- W2079425649 doi "https://doi.org/10.1016/0921-4534(94)90388-3" @default.
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