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- W2079525256 abstract "It is known that experimental parameters may affect peak characteristics in DSC studies. Kinetic parameters calculated from isothermal and dynamic runs, can also be affected by the choice of experimental conditions. The sample mass can affect the determination of reaction parameters because of the heat transport and the self-insulating properties of large masses. In the curing process of thermoset resins like unsaturated polyester crosslinked by styrene, the exothermal heat results from the reaction advance but it also produces an autocatalytic process that induces an increase in the reaction rate. The sample mass, in this kind of experiments, can influence the determination of reaction parameters not only through the effect of heat transport or thermal lag on the calorimetric results but also through the action that the sample mass exerts on the exothermal heat, and consequently, on the autocatalytic process. In this paper we intend to present the results obtained in the study of the curing kinetics of thermoset resins by DSC technique using different sample masses. We will point out that the reaction heat determined by dynamic measurement was found to be independent of the sample mass. We have obtained differences in the kinetic parameters like the reaction order, activation energy and preexponential factor when the sample mass was changed." @default.
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- W2079525256 date "1992-04-01" @default.
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- W2079525256 title "Effects of experimental sample mass on the calorimetric study of thermoset resins" @default.
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- W2079525256 doi "https://doi.org/10.1007/bf01979424" @default.
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