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• W2079546677 abstract "Porous carbon and carbide materials with different structures were characterized using adsorption of nitrogen at 77.4 K before and after preadsorption of n-nonane. The selective blocking of the microporosity with n-nonane shows that ordered mesoporous silicon carbide material (OM-SiC) is almost exclusively mesoporous whereas the ordered mesoporous carbon CMK-3 contains a significant amount of micropores (∼25%). The insertion of micropores into OM-SiC using selective extraction of silicon by hot chlorine gas leads to the formation of ordered mesoporous carbide-derived carbon (OM-CDC) with a hierarchical pore structure and significantly higher micropore volume as compared to CMK-3, whereas a CDC material from a nonporous precursor is exclusively microporous. Volumes of narrow micropores, calculated by adsorption of carbon dioxide at 273 K, are in linear correlation with the volumes blocked by n-nonane. Argon adsorption measurements at 87.3 K allow for precise and reliable calculation of the pore size distribution of the materials using density functional theory (DFT) methods." @default.
• W2079546677 created "2016-06-24" @default.
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• W2079546677 date "2013-06-06" @default.
• W2079546677 modified "2023-10-18" @default.
• W2079546677 title "Textural Characterization of Micro- and Mesoporous Carbons Using Combined Gas Adsorption and <i>n</i>-Nonane Preadsorption" @default.
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• W2079546677 doi "https://doi.org/10.1021/la401206u" @default.
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• W2079546677 hasPublicationYear "2013" @default.
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