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• W2079584489 abstract "Copper(II) complexes of general empirical formulae, [Cu(NNS)X] · xH2O (NNS = uninegatively charged tridentate ligand formed by condensation of 6-methylpyridine-2-aldehyde with thiosemicarbazide ; X = Cl, Br, NO3, and CH3COO; x= 0, 1) and [Cu(NNS)2] · 0.5H2O have been prepared and characterized by conductance, magnetic, electronic and infrared spectroscopic measurements. Magnetic and spectral data support a square-planar structure for [Cu(NNS)X] (X = Cl, Br, NO3, CH3COO) and a distorted octahedral structure for [Cu(NNS)2] · 0.5H2O. The crystal and molecular structure of [Cu(NSS)Cl] has been determined by X-ray diffraction. This complex has a distorted square-planar geometry with the copper(II) ion lying in an approximate plane of four coordinating atoms, three of which come from the 6-methylpyridine-2-carboxaldehyde thiosemicarbazone and the fourth coordination site is occupied by the chloride ligand. The thiosemicarbazone is present as the thiolate form and is coordinated to the copper(II) ion via the pyridine nitrogen atom, the azomethine nitrogen atom and the mercaptide sulfur atom. Copyright © 1996 Elsevier Science Ltd" @default.
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• W2079584489 date "1996-06-01" @default.
• W2079584489 modified "2023-09-23" @default.
• W2079584489 title "The preparation and characterization of some copper(II) Complexes of the 6-methyl-2-formylpyridine thiosemicarbazone and the x-ray crystal structure of the chloro(6-methyl-2-formylpyridinethiosemicabazonato) copper(II) complex" @default.
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• W2079584489 doi "https://doi.org/10.1016/0277-5387(96)00003-4" @default.
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