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- W2079586995 abstract "[2.1.1]Orthocyclophanes 2 are prepared by pyrolysis of the corresponding 2-thia[3.1.1]orthocyclophane 2,2-dioxides 9, which are prepared by the reaction of 1,2-bis(2-bromomethylbenzyl)benzenes 7 with Na2S in ethanol under high dilution conditions, followed by oxidation with m-chloroperbenzoic acid. The conformational studies on [2.1.1]orthocyclophanes 2, which adopt flexible saddle and crown structures in comparison with the corresponding 10,15-dihydro-5H-tribenzo[a,d,g]cyclononene ([1.1.1]orthocyclophane) 1, are discussed." @default.
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- W2079586995 date "2001-01-01" @default.
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- W2079586995 title "Medium-sized cyclophanes. Part 55. Synthesis and conformational studies of [2.1.1]orthocyclophanes" @default.
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- W2079586995 doi "https://doi.org/10.1039/b008258i" @default.
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