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• W2079589383 abstract "Acid-promoted, selective production of 5-hydroxymethylfurfural (HMF) under high fructose concentration conditions was achieved in ionic liquids (ILs) at 80 °C. A HMF yield up to 97% was obtained in 8 min using 1-butyl-3-methylimidazolium chloride ([C4mim]Cl) catalyzed with 9 mol % hydrochloric acid. More significantly, an HMF yield of 51% was observed when fructose was loaded at a high concentration of 67 wt % in [C4mim]Cl. Water content below 15.4% in the system had little effect on HMF yield, whereas a higher water content was detrimental to both reaction rate and HMF yield. In situ NMR analysis suggested that the transformation of fructose to HMF was a highly selective reaction that proceeded through the cyclic fructofuranosyl intermediate pathway. This work increased our capacity to produce HMF, and should be valuable to facilitate cost-efficient conversion of biomass into biofuels and bio-based products." @default.
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• W2079589383 date "2010-09-01" @default.
• W2079589383 modified "2023-10-17" @default.
• W2079589383 title "Production of 5-hydroxymethylfurfural in ionic liquids under high fructose concentration conditions" @default.
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• W2079589383 doi "https://doi.org/10.1016/j.carres.2010.07.003" @default.
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