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- W2079632937 abstract "Heating rate and particle size distribution may affect peak parameters in quantitative DSC. We studied these effects with a factorial design using as test substances adipic acid (melt without noticeable decomposition), naphazoline nitrate (melt with decomposition), potassium nitrate (solid-solid transition) and sodium citrate dihydrate (dehydration). A commercial heat-flux DSC equipment was used. We found that heating rate and particle size distribution have a large, and hitherto unexpected, effect on the temperature values, temperature intervals and specific enthalpy, even for the pure melt of adipic acid. Therefore it was concluded that heating rate and particle size distribution should be standardized if accurate quantitative data are required, such as in the determination of transition temperatures and enthalpies, kinetic parameters and molar impurity." @default.
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- W2079632937 date "1982-04-01" @default.
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- W2079632937 title "Effects of heating rate and particle size on temperatures and specific enthalpies in quantitative differential scanning calorimetry" @default.
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- W2079632937 doi "https://doi.org/10.1016/0040-6031(82)85070-3" @default.
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