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- W2079685044 abstract "Abstract Novel poly(3,4‐ethylenedioxythiophene) (PEDOT) polymers bearing imidazolium‐ionic liquid moieties were synthesized by electrochemical polymerizations. For this purpose, new functional monomers were synthesized having an 3,4‐ethylenedioxythiophene (EDOT) unit and an imidazolium‐ionic liquid with different anions such as tetrafluoroborate (BF ), bis(trifluoromethane)sulfonimide ((CF 3 SO 2 ) 2 N − ), and hexafluorophosphate (PF ). Next, polymer films were obtained by electrochemical synthesis in dicholoromethane solutions. Obtained polymers were characterized, revealing the characteristics of PEDOT in terms of electrochemical and spectroelectrochemical properties, FTIR, 1 H NMR, and AFM microscopy. Interestingly, the hydrophobic character of electropolymerized films could be modified depending on the anion type. The hydrophobicity followed the trend PF > (CF 3 SO 2 ) 2 N − > BF > pure PEDOT as determined by water contact angle measurements. Furthermore, the polymers could be dissolved in a range of polar organic solvents such as dimethylformamide, propylene carbonate, and dimethyl sulfoxide making these polymers interesting candidates for wet processing methods. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 3010–3021, 2009" @default.
- W2079685044 created "2016-06-24" @default.
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- W2079685044 date "2009-05-08" @default.
- W2079685044 modified "2023-10-17" @default.
- W2079685044 title "Electrochemical synthesis of PEDOT derivatives bearing imidazolium-ionic liquid moieties" @default.
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- W2079685044 doi "https://doi.org/10.1002/pola.23384" @default.
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