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• W2079726173 abstract "We report a new synthesis of the seleno-bis (S-glutathionyl) arsinium anion, [(GS)2AsSe]−. An aqueous solution of bis-glutathionylarsenous acid, (GS)2AsOH, prepared from stoichiometric glutathione and arsenite, was reacted in situ with a solution of sodium hydrogen selenide, prepared from elemental selenium and sodium borohydride. Analysis of the arsenic and selenium K-edge X-ray absorption spectra indicated virtually quantitative formation of [(GS)2AsSe]−, with AsSe and AsS distances of 2.31 and 2.25 A, respectively, and the concentrated sample allowed a definitive X-ray spectroscopic characterization. Size-exclusion chromatography was used to separate [(GS)2AsSe]− from residual borate in the reaction mixture." @default.
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• W2079726173 date "2002-05-01" @default.
• W2079726173 modified "2023-10-16" @default.
• W2079726173 title "Synthesis, X-ray absorption spectroscopy and purification of the seleno-bis (S-glutathionyl) arsinium anion from selenide, arsenite and glutathione" @default.
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• W2079726173 doi "https://doi.org/10.1016/s0022-328x(02)01192-0" @default.
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