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- W2079759309 abstract "Contrary to the reaction of 2,2-dialkyl-1-oxa-3-aza-2-stannacyclopentane with carbon disulfide at room temperature which yields oxazolidine-2-thione and dialkyltin sulfide, the reaction of N-substituted 2,2-dialkyl-1-oxa-3-aza-2-stannacyclopentane gave a stable 1/1 adduct of carbon disulfide across the SnN bond at 0°, and afforded a mixture of thiazolidine-2-thione and oxazolidine-2-thione at moderate reaction temperature. Phenyl isothiocyanate reacted with 3-methyl-2,2-dibutyl-1-oxa-3-aza-2-stannacyclopentane to form 2-phenylimino-1,3-thiazolidine and -oxazolidine. The unusual effect of N-methyl substituent in the dialkyl-1-oxa-3-aza-2-stannacyclopentane is reported. 1,3-Dimethyl-2-dibutyl-1,3-diaza-2-stannacyclopentane reacted with carbon disulfide at 0° to give N,N′-dimethylimidazolidine-2-thione and a small amount of the 1/2 adduct which could not be converted to the imidazolidine-2-thione but to an insoluble matter by heating it in vacuo at 150°." @default.
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- W2079759309 date "1973-03-01" @default.
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- W2079759309 title "Reactions of 2,2-dialkyl-1-oxa-3-aza-2-stannacyclopentanes and 2,2-dialkyl-1,3-diaza-2-stannacyclopentanes with carbon disulfide and phenyl isothiocyanate" @default.
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- W2079759309 doi "https://doi.org/10.1016/s0022-328x(00)95096-4" @default.
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