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• W2079769698 abstract "Abstract The iodocarbonyl anion of iridium(III), [Ir(CO)2I4]−, was isolated and characterized as the isoquinolinium salt during carbonylation of ethanol and higher alcohols using IrCl3 · 3H2O as a catalyst precursor with HI as a promoter. X-ray analysis shows the presence of discrete cationic [C11H12N]+ and cis anionic species [lr(CO)2I4]−, with a distorted octahedral environment around iridium and average Ir—I and Ir—C distances of 2.702(2) and 1.86(4) A, respectively. Spectral and electrochemical studies on the intermediates isolated during carbonylation of other higher alcohols revealed a strong influence of the counter cation on the electron-transfer processes in these halocarbonyl complex of IrIII" @default.
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• W2079769698 date "1996-06-01" @default.
• W2079769698 modified "2023-09-27" @default.
• W2079769698 title "Catalytic intermediates in carbonylation reactions—III. Isolation, spectroscopy, electrochemical characteristics and crystal structure of isoquinolinium dicarbonyl tetraiodo iridium(III)" @default.
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• W2079769698 doi "https://doi.org/10.1016/0277-5387(95)00471-8" @default.
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