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• W2079777652 abstract "The reaction between NiO and (0001)- and (1bar102)-oriented Al2O3 single crystals has been investigated on model experimental systems by using the ReflEXAFS technique. Depth-sensitive information is obtained by collecting data above and below the critical angle for total reflection. A systematic protocol for data analysis, based on the recently developed CARD code, was implemented, and a detailed description of the reactive systems was obtained. In particular, for (1bar102)-oriented Al2O3, the reaction with NiO is almost complete after heating for 6 h at 1273 K, and an almost uniform layer of spinel is found below a mixed (NiO + spinel) layer at the very upmost part of the sample. In the case of the (0001)-oriented Al2O3, for the same temperature and heating time, the reaction shows a lower advancement degree and a residual fraction of at least 30% NiO is detected in the ReflEXAFS spectra." @default.
• W2079777652 created "2016-06-24" @default.
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• W2079777652 date "2014-01-10" @default.
• W2079777652 modified "2023-10-01" @default.
• W2079777652 title "Studying the surface reaction between NiO and Al₂O₃<i>via</i>total reflection EXAFS (ReflEXAFS)" @default.
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• W2079777652 doi "https://doi.org/10.1107/s1600577513031299" @default.
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