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- W2079778844 abstract "Abstract The fabrication of AlN-(Y2O3) matrix ceramics reinforced with dispersed TiN or TiB2 particles is described and the resulting specimens are characterized by their mechanical properties and thermal conductivity. The microstructures of the TiN-reinforced specimens sintered at 1700 °C without isothermal hold show homogeneously distributed TiN particles (≈ 1 μm) in the fine-grained (1–2 μm) AlN matrix. In contrast, the coarse TiB2 grains (2–3 μm) of the specimens sintered at 1750 °C for 60 min are distributed inhomogeneously in the AlN matrix. Furthermore, the surface of the TiB2 grains reacted to TiN and BN during densification in 0.1 M Pa N2. The mechanical properties of the AlN- (0.5 wt% Y 2 O 3 ) 5 wt% TiN composites sintered at 1700 °C without holding time were determined to be 12.5 GPa, 390 MPa and 3.6 MPa m 1 2 for the Vickers hardness HV, the four-point bending strength σB and the fracture toughness KIc, respectively. The AlN- (4 wt% Y 2 O 3 ) 25 wt% TiN specimen sintered at 1900 °C for 60 min gave 10.7 GPa for the Vickers hardness and 270 MPa for the four-point bending strength. The fracture toughness was determined to be 8.3 MPa m 1 2 . In addition, the thermal conductivity of the AlN-TiN composites was of the order of 65 and 105 W m−1 K−1 for composites sintered at 1700 °C without isothermal hold and at 1900 °C for 60 min, respectively. The AlN- (2 wt% Y 2 O 3 ) 10 wt% TiB2-containing specimen sintered at 1750 °C for 60 min has HV of 9.5 GPa, σB of 220 MPa and KIc of 3.7 MPa m 1 2 . The influence of fracture mode and intrinsic stresses on the mechanical properties is illustrated and discussed. Finally, the processing of AlN-(4 wt% Y2O3) ceramics without reinforcing particles coated with the TiN-particle reinforced AlN is reported. These layered materials exhibit a high thermal conductivity of 150 W m−1 K−1 inside the body and enhanced hardness, fracture strength and fracture toughness at the surface." @default.
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- W2079778844 date "1997-01-01" @default.
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- W2079778844 title "Processing and properties of AlN matrix composite ceramics containing dispersed hard materials" @default.
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- W2079778844 doi "https://doi.org/10.1016/s0955-2219(97)88017-x" @default.
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