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- W2079799486 abstract "A Ethylene glycol dimethacrylate (EGDMA) methacrylic acid (MAA) resin was used for preconcentration of lead at trace levels in water samples. For this purpose, a flow-injection, solid phase extraction method was developed for the determination of lead by flame atomic absorption spectrometry. Lead ions were sorbed on a EGDMA–MAA column at pH 4, followed by an elution step using 288 µL of 4.0 M nitric acid solution and determination by flame atomic absorption spectrometry. Optimum conditions for quantitative sorption involving the pH, sample volume, loading and elution flow rates, eluent type, and volume were investigated. A 868-fold enrichment factor could be reached. The detection limit for the water samples, estimated from the noise on the signal obtained for 250 mL of 10 µg L−1 loaded at 4.9 mL min−1 was 1.04 µg L−1. The method was applied for lead determination in river water samples collected in Edirne, Turkey. Recoveries of spiked solutions (10 µg L−1) to river water samples were quantitative. Finall..." @default.
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- W2079799486 date "2009-10-01" @default.
- W2079799486 modified "2023-09-26" @default.
- W2079799486 title "Online solid phase preconcentration using EGDMA–MAA copolymer for lead determination by FAAS" @default.
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- W2079799486 doi "https://doi.org/10.1080/02772240802631899" @default.
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