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• W2079850700 abstract "We isolated a mixture of glyco-peptidolipids (mycosides C) from a non-photochromogenic atypical strain of Mycobacteria. The main component, mycoside C1217, contains a 3 D-hydroxyacid with 28 carbons, two 6-deoxysugars and four amino compounds. The two sugars are 6-deoxytalose and trimethylrhamnose (a minor component contains 3,4-dimethylrhamnose instead of trimethylrhamnose). The four amino compounds are three aminoacids, phenylalanine, allothreonine and alanine, plus an aminoalcool identified with alaninol by gas chromatography of the N-trifluoracetyl derivative. The phenylalanine is N-terminal in the peptide, and linked to the fatty acid by an amide bond. We established, by β-elimination in alkaline medium, that the deoxytalose is linked to the hydroxyl of the allo-threonine by a glycosidic bond. After a mild hydrolysis of the mycoside, we isolated a glycopeptide containing allo-threonine, alanine, alaninol and trimethylrhamnose. By use of the dimethylamino-naphtalene sulfonyl method end of Edman degradation, we have shown that the sequences of this glycopeptide is: allo-threonyl-alanyl-alaninol-trimethylrhamnose All these results, along with those obtained from some other reactions, support the following structure for the mycoside C1217, which is in agreement with mass spectrometric results:" @default.
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• W2079850700 date "1968-09-01" @default.
• W2079850700 modified "2023-10-17" @default.
• W2079850700 title "Structure d'un glycoside de peptidolipide isole d'une mycobacterie" @default.
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• W2079850700 doi "https://doi.org/10.1111/j.1432-1033.1968.tb00396.x" @default.
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