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- W2079883998 abstract "A new type of crystal of glycylglycine (GlyGly) hydrate was crystallized from an aqueous solution, and the structure of the crystal has been determined by x-ray diffraction. The crystal is monoclinic, and the space group is C2/c, with the cell constants of a = 15.941(2) Å, b = 4.774(2) Å, c = 19.428(2) Å and β = 109.884(7)° at 296 K. There are eight GlyGly molecules and six water solvent in the cell. The GlyGly molecules are packed in a parallel β-sheet arrangement. The single crystal was obtained with a maximum size of 10 × 7 × 4 mm and is not stable under atmospheric conditions. The transparent crystal turned to turbid with the elapse of time. The isotropic 13C chemical shifts obtained from the 13C cross polarization magic angle spinning nmr experiments reveal that GlyGly hydrate was changed into GlyGly (form α) by dehydration. © 1998 John Wiley & Sons, Inc. Biopoly 45: 333–339, 1998" @default.
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- W2079883998 date "1998-04-05" @default.
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- W2079883998 title "Structure of GlyGly peptide in the crystalline state as studied by X-ray diffraction and solid state13C-NMR methods" @default.
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- W2079883998 doi "https://doi.org/10.1002/(sici)1097-0282(19980405)45:4<333::aid-bip7>3.0.co;2-m" @default.
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