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- W2079891385 abstract "Abstract The composition and structure of the main decomposition product of Bi-2212 annealed under high oxygen pressures was determined by WDS, TEM and XRD analyses. The high pressure decomposition reaction for Bi-2212 can be written as: Bi2Sr2Ca1Cu2O8 + δ+O2→0.754(Bi2Sr2.48Ca1.19Oy) + 0.246(Bi2Sr0.53Ca0.39Ox) + 2CuO The highly oxidised phase Bi2Sr2.48Ca1.19Oy has the same composition as a less oxidised phase whose solid solution region was found to be centred on the Bi:(Sr + Ca) 1:2 or (Bi + Cu):(Sr + Ca) 9:(11 + 5) positions. The average atomic positions of the high pressure phase have been determined by high resolution images and image simulations along [110] and [001] directions with different sample thickness. In addition, experimental XRD has been compared with calculated XRD data for possible structures of the phase. The average structure was confirmed to be a perovskite-like structure with Sr occupying A-sites and Bi and Ca occupying B-sites. The average occupancy of Bi and Sr positions is 0.75 and the other positions were occupied by both Ca and Bi ions with an occupancy of 0.5 for Ca and 0.25 for Bi." @default.
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- W2079891385 date "1996-08-01" @default.
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- W2079891385 title "Identification of the high pressure phase in BiSrCaCuO superconductors by HRTEM and XRD" @default.
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- W2079891385 doi "https://doi.org/10.1016/0921-4534(96)00366-8" @default.
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