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- W2080135239 abstract "[Me 3 PhN][ClO 4 ], [Me 3 PhN][BF 4 ], [MePh 3 P] [ClO 4 ], and [MePh 3 P][BF 4 ] were synthesized and their structures and thermodynamic data of transitions were determined. [Me 3 PhN][ClO 4 ]: P2 1 /c, a= 852.7(3) pm, b= 580.9(2) pm, c=2260.1(8) pm, β =96.65(3)° and Z= 4. [Me 3 PhN][BF 4 ]: P2 1 2 1 2 1 , a= 584.82(8) pm, b= 835.04(8) pm, c=2258.5(2) pm, and Z=4. [MePh 3 P]·[ClO 4 ]: P2 1 /c, a= 1491.0(3) pm, b= 1378.6(1) pm, c= 1791.6(2)pm, β = 90.66(1)° and Z= 8. [MePh 3 P] ·[BF 4 ]: P2 1 /c, a=1487.4(2)pm, b= 1377.5(1)pm, c= 1768.7(1)pm, β = 91.00(1)° and Z= 8. Two solid-solid phase transitions were detected in DSC for both trimethylphenylammonium compounds. Modification III of [Me 3 PhN][BF 4 ] and the modification II of [Me 3 PhN][ClO 4 ] are isotypic. The latter phase has lattice parameters of a= 2260.6(7) pm, b= 852.7(3) pm, and c= 586.3(2) pm at 373 K. No phase transitions were observed in the phosphonium compounds in the range 153-600 K." @default.
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- W2080135239 date "2000-01-01" @default.
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- W2080135239 title "Crystal structures and DSC investigations of trimethylphenylammonium perchlorate, trimethyl-phenylammonium tetrafluoroborate, methyltriphenyl-phosphonium perchlorate, and methyltriphenyl-phosphonium tetrafluoroborate, [Me<sub>3</sub>PhN][ClO<sub>4</sub>], [Me<sub>3</sub>PhN][BF<sub>4</sub>], [MePh<sub>3</sub>P][ClO<sub>4</sub>], and [MePh<sub>3</sub>P][BF<sub>4</sub>]" @default.
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- W2080135239 doi "https://doi.org/10.1524/zkri.2000.215.1.52" @default.
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