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- W2080201145 abstract "Capillary zone electrophoresis (CZE) is presented as a new tool to resolve and analyze the ultimate degradation products of poly(d,l-lactic acid) aliphatic polyesters, namely water-soluble oligomers with a degree of polymerization lower than 8. The investigated oligomers were those present in a concentrated commercial d,l-lactic acid solution and those obtained by concentration of the same solution under vacuum. The repeatability of peak migration time was increased by introducing a relative migration factor aimed at minimizing the run-to-run peak shifts which depend on the experimental conditions, especially on the capillary and even on the instrument. Ring-opening of d,l-lactide was used to assign CZE peaks due to lactoyllactate and lactate. The rate constant and the activation energy of lactoyllactate hydrolysis were determined by monitoring the formation of lactate by CZE." @default.
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- W2080201145 date "1995-09-01" @default.
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- W2080201145 title "Monitoring of the poly(d,l-lactic acid) degradation by-products by capillary zone electrophoresis" @default.
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- W2080201145 doi "https://doi.org/10.1016/0021-9673(95)00517-q" @default.
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