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- W2080207118 abstract "A fully automated, qualitative screening HPLC method for the identification of basic compounds in urine has been developed. A 1-ml volume of urine was extracted by on-line extraction and separated on two coupled strong cation-exchange (SCX) columns (2 × LunaSCX, 150 mm × 4.6 mm, 5 μm) under isocratic conditions. The mobile phase consisted of a mixture of potassium dihydrogenphosphate buffer (pH 2.3) and acetonitrile. The use of photodiode-array detection (DAD, λ = 190–800 nm) gave access to a library of approximately 2600 toxicologically relevant compounds. The validated method is reliable, simple and in addition successfully proven with the analysis of real biological specimen for the routine use." @default.
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- W2080207118 date "2006-11-01" @default.
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- W2080207118 title "New screening method for basic compounds in urine by on-line extraction–high-performance liquid chromatography with photodiode-array detection" @default.
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- W2080207118 doi "https://doi.org/10.1016/j.chroma.2006.09.009" @default.
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