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- W2080242889 abstract "Subsequent addition of 1,2-benzenedithiol (S 2 –H 2 ) and n BuLi to a solution of [Ru(NO)Cl 3 · x MeOH] in THF afforded exclusively the monomeric species NBu 4 [Ru II (NO)(S 2 ) 2 ] ( 1 ). Formation of dimeric (NBu 4 ) 2 [Ru II (NO)(S 2 ) 2 ] 2 ( 2 ) has been confirmed when the deprotonated ligand S 2 –Li 2 was added to [Ru(NO)Cl 3 · x MeOH] and allowed to stir for 30 h. The monomer 1 undergoes aerial oxidation to give (NBu 4 ) 2 [Ru IV (S 2 ) 3 ] ( 3 ). The reaction between RuCl 3 · x H 2 O and S 2 –H 2 in the presence of NaOMe, afforded the dinulear Ru III species (NMe 4 ) 2 [Ru III (S 2 ) 2 ] 2 ( 4 ). A modified method for the preparation of 1 is being employed to synthesize the osmium analogue NBu 4 [Os(NO)(S 2 ) 2 ] ( 5 ) effectively. The solid state structures of 1 , 2 and 3 were determined by X-ray crystal structure analysis. A comparison of relevant bond distance data suggests that 1,2-benzenedithiolate acts as an “innocent” ligand." @default.
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- W2080242889 date "2004-09-01" @default.
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- W2080242889 title "Synthesis, structure and reactivity of complexes containing [M(S2)2] fragments (M=Ru, Os; (S2)2−=1,2-benzenedithiolate (2−))" @default.
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- W2080242889 doi "https://doi.org/10.1016/j.ica.2004.05.008" @default.
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