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- W2080301529 abstract "Palladium catalysts containing Pd(II) supported on Al2O3 and alumina-based mixed oxides, Al2O3-ZrO2, Al2O3-CeO2, and Al2O3-Fe2O3, are very effective in the Heck coupling of iodobenzene with cyclohexene in DMF solution. The best results, up to 81% of monoarylated products with a selectivity to 4-phenylcyclohexene (3) close to 90% were obtained with KOH as a base. The catalytic activity of palladium supported on alumina-based oxides was compared with that of homogeneous precursors, such as Pd(OAc)2 and PdCl2(PhCN)2, used in [Bu4N]Br as the reaction medium. Under such conditions homogeneous systems were more selective and produced up to 60% of monoarylated products with a selectivity to 3 close to 60%." @default.
- W2080301529 created "2016-06-24" @default.
- W2080301529 creator A5009922793 @default.
- W2080301529 creator A5050082783 @default.
- W2080301529 date "2010-03-25" @default.
- W2080301529 modified "2023-09-26" @default.
- W2080301529 title "Selective Heck Arylation of Cyclohexene with Homogeneous and Heterogeneous Palladium Catalysts" @default.
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- W2080301529 doi "https://doi.org/10.3390/molecules15042166" @default.
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