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- W2080302844 abstract "A liquid chromatography (LC)-based method with mass spectrometric (MS) detection was developed for simultaneous determination of various algal and cyanobacterial toxins extracted from phytoplankton occurring world-wide in marine waters and lakes. The method enables quantification of saxitoxin, anatoxin-A, domoic acid, nodularin, microcystins, okadaic acid and dinophysistoxin-1 with a single chromatographic run. In addition, the applied chromatographic conditions allow isolation and identification of substances suspected to be new microcystins (cyclic peptides) by fraction collection, hydrolysis, derivatisation of resulting free amino acids with the modified chiral Marfey's reagent N-alpha-(2,4-dinitro-5-fluorophenyl)-L-valinamide (L-FDVA) and enantioselective analysis of the amino acid derivatives by LC-ESI-MS." @default.
- W2080302844 created "2016-06-24" @default.
- W2080302844 creator A5027791185 @default.
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- W2080302844 date "2003-04-01" @default.
- W2080302844 modified "2023-10-10" @default.
- W2080302844 title "Liquid chromatography–electrospray ionisation-mass spectrometry based method for the simultaneous determination of algal and cyanobacterial toxins in phytoplankton from marine waters and lakes followed by tentative structural elucidation of microcystins" @default.
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- W2080302844 doi "https://doi.org/10.1016/s0021-9673(03)00485-0" @default.
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