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- W2080307067 abstract "Two convenient routes to 9H-tribenz[b,d,f]azepine (2) have been developed. The first method involves the deoxygenation and hydrolysis of 1,4-dihydro-1,4-epoxy-9-acetyl-9H-tribenz[b,d,f]azepine (8) employing low-valent titanium. The second method employs the reactive intermediate 10,11-didehydro-5-acetyl-5H-dibenz[b,f]azepine (7) in a Diels-Alder reaction with 1,3-cyclohexadiene. The resulting cycloadduct 13 upon undergoing a retro-Diels-Alder reaction and hydrolysis yields 2. 1-Methoxy-9H-tribenz[b,d,f]azepine (11) was prepared from ring opening of 8 to 1-hydroxy-9-acetyl-9H-tribenz[b,d,f]azepine (10) followed by methylation with dimethyl sulfate and hydrolysis" @default.
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- W2080307067 date "2010-08-22" @default.
- W2080307067 modified "2023-09-27" @default.
- W2080307067 title "ChemInform Abstract: Preparation of 9H-Tribenz(b,d,f)azepine and Its 1-Methoxy Derivative." @default.
- W2080307067 cites W2953162035 @default.
- W2080307067 doi "https://doi.org/10.1002/chin.199144216" @default.
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