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- W2080422022 abstract "By focusing on a range of fractions of medium-chain-length polyhydroxyalkanoates (mcl-PHA), a more in-depth understanding of the thermal properties and the crystalline structure has been gained. Dual-mode melting was observed for all the fractionated samples. Further DSC analysis revealed that such phenomenon was due to the presence of two crystalline phases (phase I and phase II), forming at different temperatures. As noted, for the samples with higher 3-hydroxytetradecanoate (HTD) comonomer composition, the crystallization rate of phase II was much depressed, which made phase I dominant. The WAXD and FTIR results indicate that the two phases differ in the crystalline structure. The in situ IR and WAXD registrations indicate that phase I would transform into phase II through a melting-recrystallization process during heating. The high similarity of IR spectra in the range of 1500–900 cm−1 between phases I and II excludes the possibility of adopting different conformation. It is suggested that major differences between the two crystalline phases lie in the molecular packing." @default.
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- W2080422022 date "2009-08-01" @default.
- W2080422022 modified "2023-10-08" @default.
- W2080422022 title "Polymorphic crystallization of fractionated microbial medium-chain-length polyhydroxyalkanoates" @default.
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- W2080422022 doi "https://doi.org/10.1016/j.polymer.2009.07.011" @default.
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