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• W2080441477 abstract "Oriented radicals trapped in γ-irradiated single crystals of potassium uranyl nitrate [K(UO2)(NO3)3], dipotassium uranyl nitrate [K2(UO2)(NO3)4], and diammonium uranyl nitrate [(NH4)2(UO2)(NO3)4] were investigated at room temperature using EPR. Two distinct radicals having considerable differences in g factors and negligible hyperfine structure were observed. 14N hyperfine interaction was observed only in certain orientations at low temperatures. These species were assigned to NO3 radicals trapped at the bidentate and unidentate nitrate sites available in these crystals. The assignments are based on the known behavior, the observed site splittings, and a comparison of the direction cosines of the g tensor with the crystal structure. The g shifts could be accounted for qualitatively on the basis of an orbital level scheme and the differences in the nature of bonding with the uranium atom in the anion. In the case of potassium uranyl nitrate, slight differences in the principal g factors indicate that the three bidentate nitrates of the anion are not identical." @default.
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• W2080441477 date "1981-12-01" @default.
• W2080441477 modified "2023-09-25" @default.
• W2080441477 title "EPR study of the NO3 radical in irradiated K(UO2)(NO3)3, K2(UO2)(NO3)4, and (NH4)2(UO2(NO3)4 single crystals" @default.
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• W2080441477 doi "https://doi.org/10.1016/0022-2364(81)90149-9" @default.
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