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• W2080461387 startingPage "2627" @default.
• W2080461387 abstract "Reduction of trace polycyclic aromatic hydrocarbon (PAH) byproducts in supercritical water oxidation (SCWO) of 2-chlorophenol (2CP) effected by CuO/ZSM-5 has been investigated in the present work. In the channels of ZSM-5, due to a restricted environment, formation of undesired PAH byproducts in the SCWO of 2CP was significantly suppressed. Only trace light-PAHs with a molecular size less than 6 Å were formed in the SCWO of 2CP. Carcinogenic PAHs (heavy-PAHs) were not found. Structures of CuO and Cu2O in the channels of ZSM-5 that involved in the catalytic SCWO of 2CP were studied by X-ray photoelectron spectroscopy (XPS). The Cu2O-to-CuO ratio was approximately 0.15. Existence of the Cu(I) and Cu(II) was also confirmed by the preedge X-ray absorption near edge structural (XANES) spectroscopy. The copper oxides with a square-plane structure were observed by electron paramagnetic resonance (EPR) spectra. Furthermore, the extended X-ray absorption fine structural (EXAFS) spectra suggest that the copper oxides in the channels of ZSM-5 may form Cu3O2 clusters with Cu−Cu and Cu−O bond distances of 2.79 and 1.91 Å, respectively. The Cu3O2 clusters were oxidized to Cu3O4 by H2O2 in supercritical water." @default.
• W2080461387 created "2016-06-24" @default.
• W2080461387 creator A5063689362 @default.
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• W2080461387 date "2000-02-12" @default.
• W2080461387 modified "2023-10-09" @default.
• W2080461387 title "Byproduct Shape Selectivity in Supercritical Water Oxidation of 2-Chlorophenol Effected by CuO/ZSM-5" @default.
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• W2080461387 doi "https://doi.org/10.1021/la990298a" @default.
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