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• W2080495548 abstract "In contrast to some earlier indications, various organo-uranium(IV) complexes of the general type Cp3UX (Cp = η5-C5H5; X = CH3, C2H5, i-C3H7, n-C4H9, t-C4H9, N(C2H5)2, and even P(C6H5)2 and NCBH3, but not BH4 or NCS) react in solution with CO under mild conditions, (viz. room temperature and atmospheric pressure of CO). The (IR, 1H NMR and NIR/VIS) spectroscopic properties of the (1:1) insertion products in case of X = alkyl or dialkylamide are in full accord with their formulation as dihapto-acyl and dihapto-carbamoyl complexes, respectively. While the carbenoid η2-OCX ligands are reluctant to undergo consecutive reactions typical of other oxy-carbene systems, reversible equilibria between monomers and dimers in solution (for R = CH3 and C2H5) cannot be ruled out. On the other hand, the dihapto-acyl complexes show a clean reversibility of the CO-uptake at temperatures above 60°C." @default.
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• W2080495548 date "1984-09-01" @default.
• W2080495548 modified "2023-10-03" @default.
• W2080495548 title "Facile insertion of carbon monoxide into the UC and UN bonds of some tris(cyclopentadienyl)uranium(IV)-alkyl and -dialkylamide derivatives" @default.
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• W2080495548 doi "https://doi.org/10.1016/0022-328x(84)80480-5" @default.
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