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- W2080524380 abstract "A fast and easy sample preparation procedure for analysis of acrylamide in various food matrices was developed and optimized. In its first step, deuterated acrylamide internal standard is added to 1 g of homogenized sample together with 5 mL of hexane, 10 mL of water, 10 mL of acetonitrile, 4 g of MgSO4, and 0.5 g of NaCl. Water facilitates the extraction of acrylamide; hexane serves for sample defatting; and the salt combination induces separation of water and acetonitrile layers and forces the majority of acrylamide into the acetonitrile layer. After vigorous shaking of the extraction mixture for 1 min and centrifugation, the upper hexane layer is discarded and a 1 mL aliquot of the acetonitrile extract is cleaned up by dispersive solid-phase extraction using 50 mg of primary secondary amine sorbent and 150 mg of anhydrous MgSO4. The final extract is analyzed either by liquid chromatography−tandem mass spectrometry or by gas chromatography−mass spectrometry (in positive chemical ionization mode) using the direct sample introduction technique for rugged large-volume injection. Keywords: Acrylamide; sample preparation; liquid chromatography−mass spectrometry; gas chromatography−mass spectrometry; direct sample introduction" @default.
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- W2080524380 date "2006-08-18" @default.
- W2080524380 modified "2023-10-10" @default.
- W2080524380 title "Rapid Sample Preparation Method for LC−MS/MS or GC−MS Analysis of Acrylamide in Various Food Matrices" @default.
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- W2080524380 doi "https://doi.org/10.1021/jf061330r" @default.
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