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W2080551440 abstract "3‘,3‘-Difluoro-2‘-hydroxymethyl-4‘,5‘-unsaturated carbocyclic nucleosides 1−3 have been stereoselectively synthesized from ester 10, which can be conveniently prepared from 2,3-isopropylidene-d-glyceraldehyde 7 in five steps. The whole synthesis highlighted the stereoselective Reformatskii−Claisen rearrangement, ring-closing metathesis (RCM), and palladium-catalyzed allylic alkylation, in which the regioselectivity was reversed from that of nonfluorinated substrates." @default.
W2080551440 created "2016-06-24" @default.
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W2080551440 date "2007-11-17" @default.
W2080551440 modified "2023-10-07" @default.
W2080551440 title "Synthesis of 3‘,3‘-Difluoro-2‘- hydroxymethyl-4‘,5‘-Unsaturated Carbocyclic Nucleosides" @default.
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W2080551440 doi "https://doi.org/10.1021/ol7023955" @default.
W2080551440 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/18020349" @default.
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