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- W2080558353 abstract "Research in the field of procyanidins is always hindered by the lack of procyanidin standards, and the preparation of procyanidins, especially in large scale, remains difficult and time-consuming. Commercial sources of procyanidin standards are scarce. In this study, a rapid preparation method of procyanidins by using low-pressure column chromatography was developed. Procyanidins in Granny Smith apples were extracted with boiled water and purified on an ADS-17 macroporous resin column to obtain a Granny Smith apple procyanidin extract (GSE). GSE was fractionated according to its degree of polymerization on a Toyopearl TSK HW-40s column. Procyanidins B2 (epicatechin-(4β−8)-epicatechin) and C1 (epicatechin-(4β−8)-epicatechin-(4β−8)-epicatechin) were prepared without HPLC separation. Oligomeric procyanidins from Granny Smith apples were also identified by liquid chromatography−electrospray ionization−mass spectrometry." @default.
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- W2080558353 date "2008-02-26" @default.
- W2080558353 modified "2023-10-18" @default.
- W2080558353 title "Rapid Preparation of Procyanidins B2 and C1 from Granny Smith Apples by Using Low Pressure Column Chromatography and Identification of Their Oligomeric Procyanidins" @default.
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- W2080558353 doi "https://doi.org/10.1021/jf072679x" @default.
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