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- W2080676851 abstract "With the catalysis of Zn(OTf)2, Mannich-type reactions of various aromatic hydrazones 1 with difluoroenoxysilane 2 proceeded smoothly to produce 2,2-difluoro-3-oxo-benzohydrazides in 27% –78% yields in THF or DCM under mild conditions. An unexpected monofluorination of hydrazone 1m with difluoroenoxysilane 2 was also disclosed in this paper. The first example of the asymmetric Mannich-type reaction of hydrazone 1a with difluoroenoxysilane 2 using chiral phosphine-oxazoline ligand has been reported, giving the adduct 3a in good yields and moderate enantioselectivities under mild conditions." @default.
- W2080676851 created "2016-06-24" @default.
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- W2080676851 date "2010-09-01" @default.
- W2080676851 modified "2023-09-23" @default.
- W2080676851 title "Zinc(II)-Catalyzed Mannich-type Reactions of Hydrazones with Difluoroenoxysilane and Its Application in the Synthesis of Optically Active 2,2-Difluoro-3-oxo-benzohydrazide" @default.
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- W2080676851 doi "https://doi.org/10.1002/cjoc.201090289" @default.
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