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- W2080711978 abstract "Abstract The oxidative chlorination of a number of phosphines R3P by means of phosphorus(V) chloride has been investigated in solution by means of 31P NMR spectroscopy. The usual products are the phosphorane R3PCl2 from the 1:1 reaction and the hexachlorophosphate R3PCl+PCl6− from the 1:2 reaction, except where complications arise from the insolubility of one of the products. In some cases one (or both) of these compounds has been isolated. Phosphines are also oxidised by PCl4+SbCl6− to form R3PCl+SbCl6− salts. The advantages and disadvantages of these reagents as chlorinating agents are discussed." @default.
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- W2080711978 date "1976-01-01" @default.
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- W2080711978 title "Phosphorus pentachloride as a chlorinating agent" @default.
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- W2080711978 doi "https://doi.org/10.1016/0022-1902(76)90004-x" @default.
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