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- W2080759718 abstract "A high-heating-rate, thermoanalytical technique was developed and applied in an investigationof the pyrolysis and oxidation of nine polymeric fuel binders typical of those used in composite propellants. The experimental method permitted detection and measurement of energy effects from reactions in samples heated nearly uniformly at rates from 50° to 300°K/sec. Tests were performed at pressures from 0.02 to 6.85 atm. The results of the high-heating-rate pyrolysis tests in a neutral atmosphere were different from those obtained by conventional laboratory techniques at low heating rates. Although in either case the energy effects were small compared to oxidation effects, a change in the pyrolysis mechanism with heating rate was apparent. Tests in which the polymers were oxidized either with gaseous oxygen or by the decomposition products of admixed ammonium perchlorate showed evidence of an exothermic reaction at a temperature 100° to 150°K below the sample ignition temperature. Although significant heating resulted from this reaction, it apparently became reactant limited and may be an essential precursor to the strongly exothermic runaway ignition reaction." @default.
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- W2080759718 date "1973-01-01" @default.
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- W2080759718 title "Pyrolysis and oxidation of polymers at high heating rates" @default.
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- W2080759718 doi "https://doi.org/10.1016/s0082-0784(73)80105-5" @default.
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