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• W2080771387 abstract "Abstract Highly dispersed and near stoichiometric chalcopyrite CuInSe 2 nanoparticles were successfully synthesized via a facile and rapid one-pot method. For understanding the reaction pathway, the solid intermediates obtained at different stages of CuInSe 2 nanoparticles synthesis process were investigated in detail by powder X-ray diffraction (XRD), X-ray photoelectron spectrometer (XPS), energy dispersive spectroscopy (EDS) and Raman spectroscopy. The XRD patterns showed that the phase formation sequence was CuSe → CuInSe 2 . The XPS results indicated that the valences of Cu and Se in CuSe were +1 and −1, respectively. The chemical composition of the solid intermediates revealed the presence of the solid-state In–Se secondary phases in the synthesis process. However, no XRD signals or Raman signals of the solid-state In–Se secondary phase were observed. Based on the experimental results, the possible reaction pathway was proposed." @default.
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• W2080771387 date "2013-10-01" @default.
• W2080771387 modified "2023-10-13" @default.
• W2080771387 title "Synthesis and reaction pathway investigation of chalcopyrite CuInSe2 nanoparticles for one-pot method" @default.
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• W2080771387 doi "https://doi.org/10.1016/j.spmi.2013.07.023" @default.
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