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- W2080866093 abstract "Abstract The capability of Et4todit (title ligand) to coordinate through the two CS groups forced at very distant positions has been used to prepare some new ligand-bridged polymeric complexes, having stoichiometry M(II)Et4toditX2 (M(II) = Zn, Cd, Hg; X=Cl, Br). IR spectral results show that the ligand binds via thionic sulphur in all isolated compounds, and the low frequency spectrum of (CdEt4toditX2)n gives a different pattern from the rest, which all are very similar and consistent with a tetrahedral stereochemistry. The X-ray structure of (CdEt4toditCl2)n shows that the crystals are orthorhombic, space group P21212, a=14.199(4), b=15.550(4), c= 10.575(3) A, Z=4. Solution and refinement of the structure gave final residuals R=0.0461 and Rw=0.0615 using 1402 observed reflections. Coordination around the metal is trigonal-bipyramidal. Apical sites are occupied by Cl atoms (Cl(1) and Cl(2)). Both bidentate ligand and Cl(2) are bridging to form a polymeric tridimensional structure." @default.
- W2080866093 created "2016-06-24" @default.
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- W2080866093 date "1990-04-01" @default.
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- W2080866093 title "Complexes of 4,5,6,7-Tetrathiocino[1,2-b:3,4-b′]diimidazolyl-1,3,8,10-tetraethyl-2,9-dithione (Et4todit) with group IIb metal halides. Crystal and molecular structure of (Cd(II)Et4toditCl2)n" @default.
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- W2080866093 doi "https://doi.org/10.1016/s0020-1693(00)80482-x" @default.
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