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- W2080884883 abstract "Mononuclear cryptates of Pb2+, Cd2+ and Hg2+ with the small host 1,4,7,10,13,16,21,24-octaazabicyclo[8.8.8]hexacosa-4,6,13,15,21,23-hexaene (imBT) showed satellite peaks in 1H NMR solution spectra throughout the accessible (–40 to +70 °C) fluid range of solvents used indicating kinetic inertness toward decomplexation. Solid-state MAS NMR studies were made on these cryptates and on dinuclear silver(I) and copper(I) analogues, in the latter case establishing coupling of 63,65Cu to 15N. A crystal structure determination of the mercury cryptate showed a symmetrical six-co-ordinate site for Hg2+ with all imino nitrogens co-ordinated, consistent with the observation, for the isomorphous cadmium(II) complex, of a 13-line 113Cd resonance in the CP MAS NMR spectrum." @default.
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- W2080884883 date "1999-01-01" @default.
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- W2080884883 title "Kinetically inert cryptate systems: solid state and solution NMR studies †" @default.
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- W2080884883 doi "https://doi.org/10.1039/a806791k" @default.
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