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- W2080917296 abstract "Abstract Several fully protected tri- and pentapeptides containing a central symmetrical α,α-dialkyl glycine residue, with the alkyl group varying from methyl or ethyl to benzyl, were synthesized in good yields by a strategy based on the Ugi–Passerini reaction. Each Ugi–Passerini adduct was selectively cleaved and the product submitted to an assisted N , N ′-dicyclohehylcarbodiimide coupling to an amino acid or dipeptide ester, respectively. Tripeptides as the above but containing a 4-methoxybenzyl group at the nitrogen atom of the central residue were also synthesized in fair to good yields by N -[(1 H -benzotriazol-1-yl)-(dimethylamino)methylene]- N -methylmethanaminium hexafluorophosphate N -oxide assisted couplings. The results reported here show that our strategy is appropriate for routine synthesis of peptides incorporating these moieties." @default.
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- W2080917296 date "2009-11-01" @default.
- W2080917296 modified "2023-10-09" @default.
- W2080917296 title "Straightforward, racemization-free synthesis of peptides with fairly to very bulky di- and trisubstituted glycines" @default.
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- W2080917296 doi "https://doi.org/10.1016/j.tet.2009.09.022" @default.
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