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- W2080928362 abstract "Six laboratories currently using pyrolysis-mass spectrometry (Py-MS) on a routine basis have participated in a collaborative exercise to assess the degree of qualitative reproducibility which can be achieved by this technique. Each laboratory has analysed six samples chosen to reflect as far as possible the diversity of samples currently examined by Py-MS. The participants analysed the samples under the conditions they felt appropriate to yield mass programs at both 70 eV and at low (⩽ 20 eV) electron energy. The results have shown that there is a measure of agreement between all laboratories for synthetic polymers but a divergence in the results is apparent as the samples become more complex. It would appear that the nature of the pyrolysis system rather than the mass spectrometer is the major factor affecting reproducibility. Undoubtedly, the problems associated with reproducing low electron energies from instrument to instrument also play a significant role." @default.
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- W2080928362 date "1985-04-01" @default.
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- W2080928362 title "Results of a pyrolysis-mass spectrometry interlaboratory trial" @default.
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