Matches in SemOpenAlex for { <https://semopenalex.org/work/W2080931826> ?p ?o ?g. }
Showing items 1 to 84 of
84
with 100 items per page.
- W2080931826 endingPage "107" @default.
- W2080931826 startingPage "99" @default.
- W2080931826 abstract "A simple method has been developed for the simultaneous determination of triclabendazole and its metabolites (sulphoxide and sulphone) in bovine milk by reversed-phase high-performance liquid chromatography (HPLC). A milk sample was homogenized with sodium sulfate anhydrous and acetonitrile, and centrifuged. The supernatant was isolated, rinsed with n-hexane saturated with acetonitrile, and evaporated. The residue was dissolved with 0.1 M potassium dihydrogenphosphate, and 0.1 M sodium hydrogencarbonate, and then cleaned up on a Bond Elut C18 cartridge. The three compounds were separated on a Capcell Pak C18 UG 120 (5 μm, 150×4.6 mm I.D.) column and determined by UV detection at 295 nm. The mobile phase was acetonitrile–0.05 M ammonium acetate (50:50), and the flow-rate was 0.8 ml/min at 40°C. The mean recoveries (n=4) were 89.1–95.0% with a relative standard deviation of 1.1–2.6%. The detection limits were 0.004–0.006 μg/g in milk. The proposed method was used to monitor raw milk samples for the market, and applied to the analysis of milk samples from 10 cows which had been administered with triclabendazole to control the liver fluke. The confirmation of the triclabendazole and its metabolites in the above milk sample has been achieved by electrospray LC–MS for the first time." @default.
- W2080931826 created "2016-06-24" @default.
- W2080931826 creator A5024054968 @default.
- W2080931826 creator A5025091607 @default.
- W2080931826 creator A5034414916 @default.
- W2080931826 creator A5043573908 @default.
- W2080931826 creator A5053631614 @default.
- W2080931826 creator A5065184409 @default.
- W2080931826 creator A5079074636 @default.
- W2080931826 date "2000-06-01" @default.
- W2080931826 modified "2023-09-29" @default.
- W2080931826 title "Simultaneous determination of triclabendazole and its sulphoxide and sulphone metabolites in bovine milk by high-performance liquid chromatography" @default.
- W2080931826 cites W2008743788 @default.
- W2080931826 cites W2021661615 @default.
- W2080931826 cites W2028130185 @default.
- W2080931826 cites W2043835772 @default.
- W2080931826 cites W2046546102 @default.
- W2080931826 cites W2054276495 @default.
- W2080931826 cites W2068112447 @default.
- W2080931826 cites W2068864672 @default.
- W2080931826 cites W4243227845 @default.
- W2080931826 doi "https://doi.org/10.1016/s0021-9673(00)00054-6" @default.
- W2080931826 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/10895937" @default.
- W2080931826 hasPublicationYear "2000" @default.
- W2080931826 type Work @default.
- W2080931826 sameAs 2080931826 @default.
- W2080931826 citedByCount "38" @default.
- W2080931826 countsByYear W20809318262012 @default.
- W2080931826 countsByYear W20809318262013 @default.
- W2080931826 countsByYear W20809318262014 @default.
- W2080931826 countsByYear W20809318262016 @default.
- W2080931826 countsByYear W20809318262017 @default.
- W2080931826 countsByYear W20809318262019 @default.
- W2080931826 countsByYear W20809318262021 @default.
- W2080931826 countsByYear W20809318262022 @default.
- W2080931826 countsByYear W20809318262023 @default.
- W2080931826 crossrefType "journal-article" @default.
- W2080931826 hasAuthorship W2080931826A5024054968 @default.
- W2080931826 hasAuthorship W2080931826A5025091607 @default.
- W2080931826 hasAuthorship W2080931826A5034414916 @default.
- W2080931826 hasAuthorship W2080931826A5043573908 @default.
- W2080931826 hasAuthorship W2080931826A5053631614 @default.
- W2080931826 hasAuthorship W2080931826A5065184409 @default.
- W2080931826 hasAuthorship W2080931826A5079074636 @default.
- W2080931826 hasConcept C119128265 @default.
- W2080931826 hasConcept C178790620 @default.
- W2080931826 hasConcept C179998833 @default.
- W2080931826 hasConcept C185592680 @default.
- W2080931826 hasConcept C2777077568 @default.
- W2080931826 hasConcept C2777463227 @default.
- W2080931826 hasConcept C2780782300 @default.
- W2080931826 hasConcept C43617362 @default.
- W2080931826 hasConcept C537181965 @default.
- W2080931826 hasConceptScore W2080931826C119128265 @default.
- W2080931826 hasConceptScore W2080931826C178790620 @default.
- W2080931826 hasConceptScore W2080931826C179998833 @default.
- W2080931826 hasConceptScore W2080931826C185592680 @default.
- W2080931826 hasConceptScore W2080931826C2777077568 @default.
- W2080931826 hasConceptScore W2080931826C2777463227 @default.
- W2080931826 hasConceptScore W2080931826C2780782300 @default.
- W2080931826 hasConceptScore W2080931826C43617362 @default.
- W2080931826 hasConceptScore W2080931826C537181965 @default.
- W2080931826 hasIssue "1-2" @default.
- W2080931826 hasLocation W20809318261 @default.
- W2080931826 hasLocation W20809318262 @default.
- W2080931826 hasOpenAccess W2080931826 @default.
- W2080931826 hasPrimaryLocation W20809318261 @default.
- W2080931826 hasRelatedWork W1603333022 @default.
- W2080931826 hasRelatedWork W1964259887 @default.
- W2080931826 hasRelatedWork W1998279148 @default.
- W2080931826 hasRelatedWork W2013299392 @default.
- W2080931826 hasRelatedWork W2032191029 @default.
- W2080931826 hasRelatedWork W2043512602 @default.
- W2080931826 hasRelatedWork W2084062459 @default.
- W2080931826 hasRelatedWork W2096641431 @default.
- W2080931826 hasRelatedWork W2155596957 @default.
- W2080931826 hasRelatedWork W2256031060 @default.
- W2080931826 hasVolume "882" @default.
- W2080931826 isParatext "false" @default.
- W2080931826 isRetracted "false" @default.
- W2080931826 magId "2080931826" @default.
- W2080931826 workType "article" @default.