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• W2080937044 abstract "Treatment of [Ru(η5-C5H5)(η4-C5H4O)]2(PF6)2 (1) with PR3 (PR3PBun3, PCy3, PMe3, PPhMe2, PPh2Me, PPh3) results in the formation of [Ru(η5-C5H4PR3)(η5-C5H4OH)]PF6 (3a–f) in ⩾ 95% yield. The crystal structure of [Ru(η5-C5H4PPh3)(η5-C5H4OH)]PF6 (3f) has been determined by X-ray diffraction techniques. 3f crystallizes in the monoclinic space grouop P21/c, with a=9.928(2), b=15.395(3), c=18.030(3) Å, β=99.07(1)°, V=2721.3(9) Å3, Z=4. The structure was refined to R=0.032 and Rw=0.035. [Ru(η5-C5H5)(η4-C5H4O)-(CH3CN)]PF6 (2) reacts with PR3 (PR3PBun3, PCy3, PMe3, PPhMe2) to give the same products as does 1, whereas with PPh2Me, PPh3, and P(p-Ph-OMe)3 a different pathway is observed giving [Ru(η5-C5H5)(η5-C5H3OH-2-PR3)]PF6 (4a–c) in ⩾ 95% yield." @default.
• W2080937044 created "2016-06-24" @default.
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• W2080937044 date "1994-03-01" @default.
• W2080937044 modified "2023-09-26" @default.
• W2080937044 title "Synthesis and characterization of phosphane-substituted hydroxyruthenocenes: crystal structure of [Ru(η5-C5H4PPh3)(η5-C5H4OH)]PF6" @default.
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• W2080937044 doi "https://doi.org/10.1016/0020-1693(93)03757-2" @default.
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